Collect. Czech. Chem. Commun. 2007, 72, 985-995
https://doi.org/10.1135/cccc20070985

Stereoselective Methylation of 1-(Diphenylphosphanyl)-2-[(methoxycarbonyl)methyl]ferrocene. The Crystal Structures of the Methylated Ester and Its Palladium(II) Complex with an Auxiliary 2-[(Dimethylamino)methyl]phenyl Ligand.

Martin Lamač, Ivana Císařová and Petr Štěpnička*

Department of Inorganic Chemistry, Faculty of Science, Charles University, Hlavova 2030, 128 40 Prague, Czech Republic

References

1a. Togni A., Hayashi T. (Eds): Ferrocenes: Homogeneous Catalysis, Organic Synthesis, Materials Science. VCH, Weinheim 1995.
1b. Togni A. in: Metallocenes (A. Togni and R. L. Halterman, Eds), Vol. 2, Chap. 11, pp. 685–721. Wiley-VCH, Weinheim 1998.
1c. Richards C. J., Locke A. J.: Tetrahedron: Asymmetry 1998, 9, 2377. <https://doi.org/10.1016/S0957-4166(98)00251-1>
1d. Arrayás R. G., Adrio J., Carretero J. C.: Angew. Chem., Int. Ed. 2006, 45, 7674. <https://doi.org/10.1002/anie.200602482>
2a. G = CN: Marr G., Ronayne J.: J. Organomet. Chem. 1973, 47, 417. <https://doi.org/10.1016/S0022-328X(00)81753-2>
2b. G = SO2Ph: Evans J. B., Marr G.: J. Chem. Soc., Perkin Trans. 1 1972, 2502. <https://doi.org/10.1039/p19720002502>
2c. G = Ph2P(E), where E = O and S: Marr G., Wakefield B. J., White T. M.: J. Organomet. Chem. 1975, 88, 357. <https://doi.org/10.1016/S0022-328X(00)89512-1>
3. Štěpnička P.: Eur. J. Inorg. Chem. 2005, 3787. <https://doi.org/10.1002/ejic.200500485>
4a. Štěpnička P., Císařová I.: Organometallics 2003, 22, 1728. <https://doi.org/10.1021/om020837y>
4b. Štěpnička P.: Inorg. Chem. Commun. 2004, 7, 426. <https://doi.org/10.1016/j.inoche.2003.12.028>
4c. Štěpnička P., Císařová I.: Z. Anorg. Allg. Chem. 2004, 630, 1321. <https://doi.org/10.1002/zaac.200400122>
5. Lamač M., Štěpnička P.: Inorg. Chem. Commun. 2006, 9, 319. <https://doi.org/10.1016/j.inoche.2005.12.003>
6. Lamač M., Císařová I., Štěpnička P.: Eur. J. Inorg. Chem. 2007, 2274. <https://doi.org/10.1002/ejic.200700093>
7. Kaestle K. L., Anwer M. K., Audhya T. K., Goldstein G.: Tetrahedron Lett. 1991, 32, 327. <https://doi.org/10.1016/S0040-4039(00)92619-4>
8. Gassman P. G., Schenk W. N.: J. Org. Chem. 1977, 42, 918. <https://doi.org/10.1021/jo00425a040>
9. Olah G. A., Husain A., Singh B. P., Mehrotra A. K.: J. Org. Chem. 1983, 48, 3667. <https://doi.org/10.1021/jo00169a010>
10. Štěpnička P., Lamač M., Císařová I.: Polyhedron 2004, 23, 921. <https://doi.org/10.1016/j.poly.2003.11.057>
11. Otwinowski Z., Minor W.: HKL Denzo and Scalepack Program Package. Nonius BV, Delft 1997.
12. Altomare A., Burla M. C., Camalli M., Cascarano G. L., Giacovazzo C., Guagliardi A., Moliterni A. G. G., Polidori G., Spagna R.: J. Appl. Crystallogr. 1999, 32, 115. <https://doi.org/10.1107/S0021889898007717>
13. Sheldrick G. M.: SHELXL97, Program for Crystal Structure Refinement from Diffraction Data. University of Göttingen, Göttingen 1997.
14. Spek A. L.: PLATON, A Multipurpose Crystallographic Tool. Utrecht University, Utrecht 2003, and updates. Distributed via Internet; http://www.cryst.chem.uu.nl/platon/.