Collect. Czech. Chem. Commun. 2005, 70, 1589-1603
https://doi.org/10.1135/cccc20051589

Preparation and Crystal Structure of Bis(tert-butyltetramethylcyclopentadienyl)dichlorotitanium

Lenka Lukešováa, Róbert Gyepesb, Jiří Pinkasa, Michal Horáčeka, Jiří Kubištaa, Jiří Čejkaa and Karel Macha,*

a J. Heyrovský Institute of Physical Chemistry, Academy of Sciences of the Czech Republic, Dolejškova 3, 182 23 Prague 8, Czech Republic
b Department of Inorganic Chemistry, Charles University, Hlavova 2030, 128 40 Prague 2, Czech Republic

References

1. Möhring P. C., Coville N. J.: J. Organomet. Chem. 1994, 479, 1. <https://doi.org/10.1016/0022-328X(94)84087-3>
2a. Langmaier J., Samec Z., Varga V., Horáček M., Mach K.: J. Organomet. Chem. 1999, 579, 348. <https://doi.org/10.1016/S0022-328X(99)00025-X>
2b. Gassman P. G, Macomber D. W., Hershberger J. W.: Organometallics 1983, 2, 1470. <https://doi.org/10.1021/om50004a044>
3. Gassman P. G., Winter C. H.: J. Am. Chem. Soc. 1986, 108, 4228. <https://doi.org/10.1021/ja00274a065>
4. Mach K., Varga V., Antropiusová H., Poláček J.: J. Organomet. Chem. 1987, 333, 205. <https://doi.org/10.1016/0022-328X(87)85153-7>
5a. Mach K., Raynor J. B.: J. Chem. Soc., Dalton Trans. 1992, 683. <https://doi.org/10.1039/dt9920000683>
5b. Horáček M., Gyepes R., Císařová I., Polášek M., Varga V., Mach K.: Collect. Czech. Chem. Commun. 1996, 61, 1307. <https://doi.org/10.1135/cccc19961307>
6. Varga V., Mach K., Polášek M., Sedmera P., Hiller J., Thewalt U., Troyanov S. I.: J. Organomet. Chem. 1996, 506, 241. <https://doi.org/10.1016/0022-328X(95)05758-H>
7a. Gassman P. G., Campbell W. H., Macomber D. W.: Organometallics 1984, 3, 385. <https://doi.org/10.1021/om00081a009>
7b. Hafner A., Okuda J.: Organometallics 1993, 12, 949. <https://doi.org/10.1021/om00027a052>
8. Vondrák T., Mach K., Varga V.: J. Organomet. Chem. 1989, 367, 69. <https://doi.org/10.1016/0022-328X(89)87206-7>
9. Vondrák T., Mach K., Varga V.: Organometallics 1992, 11, 2030. <https://doi.org/10.1021/om00042a017>
10. Gassman P. G., Macomber D. W., Hershberger J. W.: Organometallics 1983, 2, 1470. <https://doi.org/10.1021/om50004a044>
11. Soloveichik G. L., Gavrilov A. B., Strelets V. V.: Metalloorg. Khim. 1989, 2, 431.
12. Mach K., Varga V., Schmid G., Hiller J., Thewalt U.: Collect. Czech. Chem. Commun. 1996, 61, 1285. <https://doi.org/10.1135/cccc19961285>
13. Urazowski I. F., Ponomaryov V. I., Ellert O. G., Nifantev I. E., Lemenovskii D. A.: J. Organomet. Chem. 1988, 356, 181. <https://doi.org/10.1016/0022-328X(88)83088-2>
14. Hughes R. P., Kowalski A. S., Lomprey J. R., Rheingold A. L.: Organometallics 1994, 13, 2691. <https://doi.org/10.1021/om00019a027>
15. Venier C. G., Casserly E. W.: J. Am. Chem. Soc. 1990, 112, 2808. <https://doi.org/10.1021/ja00163a057>
16. Sitzmann H., Zhou P., Wolmershäuser G.: Chem. Ber. 1994, 127, 3. <https://doi.org/10.1002/cber.19941270102>
17a. Hitchcock P. B., Kerton F. M., Lawless G. A.: J. Am. Chem. Soc. 1998, 120, 10264. <https://doi.org/10.1021/ja981934e>
17b. Horáček M., Kupfer V., Thewalt U., Štěpnička P., Polášek M., Mach K.: Organometallics 1999, 18, 3572. <https://doi.org/10.1021/om990286k>
17c. Lukešová L., Horáček M., Štěpnička P., Fejfarová K., Gyepes R., Císařová I., Kubišta J., Mach K.: J. Organomet. Chem. 2002, 663, 134. <https://doi.org/10.1016/S0022-328X(02)01726-6>
18a. du Plooy K. E., du Toit J., Levendis D. C., Coville N. J.: J. Organomet. Chem. 1996, 508, 231. <https://doi.org/10.1016/0022-328X(95)05865-M>
18b. Schumann H., Zietzke K., Erbstein F., Weimann R.: J. Organomet. Chem. 1996, 520, 265. <https://doi.org/10.1016/0022-328X(96)06348-6>
19. Hanna T. E., Lobkovsky E., Chirik P. J.: J. Am. Chem. Soc. 2004, 126, 14688. <https://doi.org/10.1021/ja045884r>
20. Horáček M., Štěpnička P., Gyepes R., Císařová I., Tišlerová I., Zemánek J., Kubišta J., Mach K.: Chem. Eur. J. 2000, 6, 2397. <https://doi.org/10.1002/1521-3765(20000703)6:13<2397::AID-CHEM2397>3.0.CO;2-H>
21. Lukešová L., Horáček M., Štěpnička P., Gyepes R., Císařová I., Kubišta J., Mach K.: J. Organomet. Chem. 2004, 689, 1919. <https://doi.org/10.1016/j.jorganchem.2004.02.040>
22. Loukova G. V., Strelets V. V.: Collect. Czech. Chem. Commun. 2001, 66, 185. <https://doi.org/10.1135/cccc20010185>
23. Finch W. C., Anslyn E. V., Grubbs R. H.: J. Am. Chem. Soc. 1988, 110, 2406. <https://doi.org/10.1021/ja00216a012>
24. Troyanov S. I., Rybakov V. B., Varga V., Sedmera P., Mach K.: Metalloorg. Khim. 1991, 4, 1004.
25a. Varga V., Hiller J., Gyepes R., Polášek M., Sedmera P., Thewalt U., Mach K.: J. Organomet. Chem. 1997, 538, 63. <https://doi.org/10.1016/S0022-328X(96)06917-3>
25b. McKenzie T. C., Sanner R. D., Bercaw J. E.: J. Organomet. Chem. 1975, 102, 457. <https://doi.org/10.1016/S0022-328X(00)89390-0>
26. Howie R. A., McQuillan G. P., Thompson D. W.: J. Organomet. Chem. 1984, 268, 149. <https://doi.org/10.1016/0022-328X(84)80242-9>
27. Engelhardt L. M., Papasergio R. I., Raston C. L., White A. H.: Organometallics 1984, 3, 18. <https://doi.org/10.1021/om00079a005>
28. Kirschbaum K., Giolando D. M.: Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1991, 47, 2216. <https://doi.org/10.1107/S0108270191005061>
29. Winter C. H., Zhou X. X., Dobbs D. A., Heeg M. J.: Organometallics 1991, 10, 210. <https://doi.org/10.1021/om00047a051>
30. Hart S. L., Duncalf D. J., Hastings J. J., McCamley A., Taylor P. C.: J. Chem. Soc., Dalton Trans. 1996, 2843. <https://doi.org/10.1039/dt9960002843>
31. Jibril I., Abu Orabi S., Klaib S. A., Imhof W., Huttner G.: J. Organomet. Chem. 1992, 433, 253. <https://doi.org/10.1016/0022-328X(92)80151-M>
32. Evans W. J., Giarikos D. G., Ziller J. W.: J. Organomet. Chem. 2003, 688, 200. <https://doi.org/10.1016/j.jorganchem.2003.09.013>
33. Flores J. C., Wood J. S., Chien J. C. W., Rausch M. D.: Organometallics 1996, 15, 4944. <https://doi.org/10.1021/om960475s>
34. Zemánek J., Fröhlichová L., Šindelár P., Štěpnička P., Císařová I., Varga V., Horáček M., Mach K.: Collect. Czech. Chem. Commun. 2001, 66, 1359. <https://doi.org/10.1135/cccc20011359>
35. Alcock N. W., Toogood G. E., Wallbridge M. G. H.: Acta Crystallogr., Sect.C: Cryt. Struct. Commun. 1984, 40, 598. <https://doi.org/10.1107/S0108270184005011>
36. Thewalt U., Schomberg D.: J. Organomet. Chem. 1977, 127, 169. <https://doi.org/10.1016/S0022-328X(00)89707-7>
37. Lukens W. W., Jr., Smith M. R., III, Andersen R. A.: J. Am. Chem. Soc. 1996, 118, 1719. <https://doi.org/10.1021/ja953272o>
38. Antropiusová H., Dosedlová A., Hanuš V., Mach K.: Transition Met. Chem. (London) 1981, 6, 90. <https://doi.org/10.1007/BF00626113>
39. Altomare A., Burla M. C., Camalli M., Cascarano G., Giacovazzo C., Guagliardi A., Polidori G.: J. Appl. Crystallogr. 1994, 27, 435.
40. Sheldrick G. M.: SHELXL97. Program for Crystal Structure Refinement from Diffraction Data. University of Göttingen, Göttingen 1997.