Collect. Czech. Chem. Commun. 2001, 66, 52-66
https://doi.org/10.1135/cccc20010052

Air-Tight Three-Electrode Design of Coaxial Electrochemical-EPR Cell for Redox Studies at Low Temperatures

František Hartl*, Ronald P. Groenestein and Taasje Mahabiersing

Institute of Molecular Chemistry, University of Amsterdam, Nieuwe Achtergracht 166, NL-1018 WV Amsterdam, The Netherlands

References

1a. Farell I. R., Hartl F., Záliš S., Mahabiersing T., Vlček A., Jr.: J. Chem. Soc., Dalton Trans. 2000, 4323. <https://doi.org/10.1039/b005279p>
1b. Aarnts M. P., Wilms M. P., Peelen K., Fraanje J., Goubitz K., Hartl F., Stufkens D. J., Baerends E. J., Vlček A., Jr.: Inorg. Chem. 1996, 35, 5468. <https://doi.org/10.1021/ic960042h>
1c. Mevs J. M., Geiger W. E.: Organometallics 1996, 15, 2350. <https://doi.org/10.1021/om9600194>
1d. Webster R. D.: J. Chem. Soc., Perkin Trans. 2 1999, 263. <https://doi.org/10.1039/a806854b>
2a. Miholová D., Klíma J., Vlček A. A.: Inorg. Chim. Acta 1978, 27, L67. <https://doi.org/10.1016/S0020-1693(00)87231-X>
2b. Gaš B., Klíma J., Záliš S., Vlček A. A.: J. Electroanal. Chem. 1987, 222, 161. <https://doi.org/10.1016/0022-0728(87)80284-X>
2c. Miholová D., Gaš B., Záliš S., Klíma J., Vlček A. A.: J. Organomet. Chem. 1987, 330, 75. <https://doi.org/10.1016/0022-328X(87)80279-6>
2d. Ludvík J., Klíma J., Volke J., Kurfürst A., Kuthan J.: J. Electroanal. Chem. 1982, 138, 131. <https://doi.org/10.1016/0022-0728(82)87134-9>
2e. Klíma J., Volke J., Urban J.: Electrochim. Acta 1991, 36, 73. <https://doi.org/10.1016/0013-4686(91)85181-6>
3. Hartl F., Vlček A., Jr.: Inorg. Chem. 1991, 30, 3048. <https://doi.org/10.1021/ic00015a021>
4a. van Slageren J., Martino D., Kleverlaan C. J., Bussandri A. P., van Willigen H., Stufkens D. J.: J. Phys. Chem. A 2000, 104, 291. <https://doi.org/10.1021/jp001032b>
4b. Sakaguchi Y., Hayashi H., I’Haya Y. J.: J. Phys. Chem. 1990, 94, 291. <https://doi.org/10.1021/j100364a048>
5. Bagchi R. N., Bond A. M., Scholz F.: J. Electroanal. Chem. 1988, 252, 259. <https://doi.org/10.1016/0022-0728(88)80215-8>
6a. Mu X. H., Kadish K. M.: Electroanalysis 1990, 2, 15. <https://doi.org/10.1002/elan.1140020105>
6b. Macgregor S. A., McInnes E., Sorbie R. J., Yellowlees L. J. in: Molecular Electrochemistry of Inorganic, Bioinorganic and Organometallic Compounds (A. J. L. Pombeiro and J. A. McCleverty, Eds), p. 503. Kluwer Academic Publishers, Dordrecht 1993.
6c. Kaim W., Ernst S., Kasack V.: J. Am. Chem. Soc. 1990, 112, 173. <https://doi.org/10.1021/ja00157a028>
7. Webster R. D., Bond A. M., Coles B. A., Compton R. G.: J. Electroanal. Chem. 1996, 404, 303; and refs4–11 therein. <https://doi.org/10.1016/0022-0728(95)04363-2>
8. Allendoerfer R. D., Martinchek G. A., Bruckenstein S.: Anal. Chem. 1975, 47, 890. <https://doi.org/10.1021/ac60356a023>
9. Hartl F.: Inorg. Chim. Acta 1995, 232, 99. <https://doi.org/10.1016/0020-1693(94)04395-C>
10. Schroth W., Hintzsche E., Spitzner R., Stroehl D., Sieler J.: Tetrahedron 1995, 51, 13247. <https://doi.org/10.1016/0040-4020(95)00852-Y>
11. Stone K. J., Little R. D.: J. Org. Chem. 1984, 49, 1849. <https://doi.org/10.1021/jo00185a001>
12. Kleverlaan C. J., Stufkens D. J.: Inorg. Chim. Acta 1999, 284, 61. <https://doi.org/10.1016/S0020-1693(98)00278-3>
13. Duling. D. R.: J. Magn. Reson., Ser. B 1994, 104, 105. <https://doi.org/10.1006/jmrb.1994.1062>
14. Gritzner G., Kůta J.: Pure Appl. Chem. 1984, 56, 461. <https://doi.org/10.1351/pac198456040461>
15a. Krejčík M., Daněk M., Hartl F.: J. Electroanal. Chem. 1991, 317, 179. <https://doi.org/10.1016/0022-0728(91)85012-E>
15b. Hartl F., Luyten H., Nieuwenhuis H. A., Schoemaker G. C.: Appl. Spectrosc. 1994, 48, 1522. <https://doi.org/10.1366/0003702944027787>
16. Schumer F., Hennig H.: Personal communication.
17. Hennig H., Schroth W., Schumer F., Kaden H., Gelssner W., Mahabiersing T., Hartl F.: Unpublished results.
18. Tacke M., Fox. S., Cuffe L., Dunne J. P., Hartl F., Mahabiersing T.: J. Mol. Struct. 2001, 559, 331. <https://doi.org/10.1016/S0022-2860(00)00710-9>
19a. Lucia L. A., Burton R. D., Schanze K. S.: Inorg. Chim. Acta 1993, 208, 103. <https://doi.org/10.1016/S0020-1693(00)82891-1>
19b. Rossenaar B. D., Kleverlaan C. J., van de Ven M. C. E., Stufkens D. J., Vlček A., Jr.: Chem.-Eur. J. 1996, 2, 228. <https://doi.org/10.1002/chem.19960020216>
19c. Farrel I. R., Matoušek P., Kleverlaan C. J., Vlček A., Jr.: Chem.-Eur. J. 2000, 6, 1386. <https://doi.org/10.1002/(SICI)1521-3765(20000417)6:8<1386::AID-CHEM1386>3.0.CO;2-G>
20. Stufkens D. J., Aarnts M. P., Nijhoff J., Rossenaar B. D., Vlček A., Jr.: Coord. Chem. Rev. 1998, 171, 93. <https://doi.org/10.1016/S0010-8545(98)90017-0>
21. Rossenaar B. D., Hartl F., Stufkens D. J.: Inorg. Chem. 1996, 35, 6194. <https://doi.org/10.1021/ic9600947>
22a. Víchová J., Hartl F., Vlček A., Jr.: J. Am. Chem. Soc. 1992, 114, 10903. <https://doi.org/10.1021/ja00053a029>
22b. Rossenaar B. D., Stufkens D. J., Vlček A., Jr.: Inorg. Chim. Acta 1996, 247, 247. <https://doi.org/10.1016/0020-1693(95)04968-1>
23a. Stor G. J., Hartl F., van Outersterp J. W. M., Stufkens D. J.: Organometallics 1995, 14, 1115. <https://doi.org/10.1021/om00003a013>
23b. Rossenaar B. D., Hartl F., Stufkens D. J., Amatore C., Maisonhaute E., Verpeaux J.-N.: Organometallics 1997, 16, 4675. <https://doi.org/10.1021/om9702791>
23c. Hartl F., Le Floch P., Rosa P., Záliš S.: Unpublished results.
24. Klein A., Vogler C., Kaim W.: Organometallics 1996, 15, 236. <https://doi.org/10.1021/om950500e>