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Collect. Czech. Chem. Commun. 1994, 59, 374-380
https://doi.org/10.1135/cccc19940374

Constitution and HPLC Resolution of Enantiomers of the [8,4'-μ-R2N-commo-(1,2-C2B9H10)2-3-Co] Complexthe Third Isomer of Nitrogen-Bridged Bis

Jaromír Plešeka, Bohumír Grünera, Stanislav Heřmáneka, Jiří Fuseka and Hana Votavováb

a Institute of Inorganic Chemistry, Academy of Sciences of the Czech Republic, 250 68 Řež near Prague, Czech Republic
b Institute of Organic Chemistry and Biochemistry, Academy of Sciences of the Czech Republic, 166 10 Prague 6, Czech Republic

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  • Horáček Ondřej, Dhaubhadel Umang, Holub Josef, Grüner Bohumír, Armstrong Daniel W., Kučera Radim: Employment of chiral columns with superficially porous particles in chiral separations of cobalt bis (dicarbollide) and nido‐7,8‐C2B9H12(1‐) derivatives. Chirality 2023, 35, 937. <https://doi.org/10.1002/chir.23606>
  • Horáček Ondřej, Marvalová Jana, Štilcová Kristýna, Holub Josef, Grüner Bohumír, Kučera Radim: Reversed-phase chromatography as an effective tool for the chiral separation of anionic and zwitterionic carboranes using polysaccharide-based chiral selectors. Journal of Chromatography A 2022, 1672, 463051. <https://doi.org/10.1016/j.chroma.2022.463051>
  • Timofeev Sergey V., Zhidkova Olga B., Suponitsky Kyrill Yu., Anisimov Aleksei A., Sivaev Igor B., Yan Hong, Bregadze Vladimir I.: Rhodacarboranes containing σ- and π-carborane ligands. New aspects. Inorganica Chimica Acta 2021, 518, 120243. <https://doi.org/10.1016/j.ica.2020.120243>
  • Horáček Ondřej, Papajová-Janetková Monika, Grüner Bohumír, Lochman Lukáš, Štěrbová-Kovaříková Petra, Vespalec Radim, Kučera Radim: The first chiral HPLC separation of dicarba-nido-undecarborate anions and their chromatographic behavior. Talanta 2021, 222, 121652. <https://doi.org/10.1016/j.talanta.2020.121652>
  • Timofeev Sergey V., Sivaev Igor B., Prikaznova Elena A., Bregadze Vladimir I.: Transition metal complexes with charge-compensated dicarbollide ligands. Journal of Organometallic Chemistry 2014, 751, 221. <https://doi.org/10.1016/j.jorganchem.2013.08.012>
  • Kaplánek Robert, Martásek Pavel, Grüner Bohumír, Panda Satya, Rak Jakub, Masters Bettie Sue Siler, Král Vladimír, Roman Linda J.: Nitric Oxide Synthases Activation and Inhibition by Metallacarborane-Cluster-Based Isoform-Specific Affectors. J. Med. Chem. 2012, 55, 9541. <https://doi.org/10.1021/jm300805x>
  • Horáková Hana, Grüner Bohumír, Vespalec Radim: Emerging subject for chiral separation science: Cluster boron compounds. Chirality 2011, 23, 307. <https://doi.org/10.1002/chir.20918>
  • Krasnov V. P., Demin A. M., Levit G. L., Grishakov A. N., Sadretdinova L. Sh., Ol’shevskaya V. A., Glukhov I. V., Kalinin V. N., Charushin V. N.: Determination of enantiomeric purity of 1-substituted 3-amino-1,2-dicarba-closo-dodecaboranes by HPLC on chiral stationary phases. Russ Chem Bull 2008, 57, 2535. <https://doi.org/10.1007/s11172-008-0364-5>
  • Horáková Hana, Vespalec Radim: Chiral separability of hydrophobic boron cluster anions with native cyclodextrins in water–methanol background electrolytes. Electrophoresis 2007, 28, 3639. <https://doi.org/10.1002/elps.200600814>
  • Plešek Jaromı́r, Grüner Bohumı́r, Cı́sařová Ivana, Báča Jiřı́, Selucký Pavel, Rais Jiřı́: Functionalized cobalt bis(dicarbollide) ions as selective extraction reagents for removal of M2+ and M3+ cations from nuclear waste, crystal and molecular structures of the [8,8′-μ-CIP(O)(O)2(1,2-C2B9H10)2-3,3′-Co]HN(C2H5)3 and [8,8′-μ-Et2NP(O)(O)2(1,2-C2B9H10)2-3,3′-Co](HN(CH3)3). Journal of Organometallic Chemistry 2002, 657, 59. <https://doi.org/10.1016/S0022-328X(02)01325-6>
  • Bown Mark, Grüner Bohumı́r, Štı́br Bohumil, Fontaine Xavier L.R., Thornton-Pett Mark, Kennedy John D.: Eleven-vertex polyhedral metalladicarbaborane chemistry. Reactions of neutral nido-5,6-C2B8H12 and the [nido-6,9-C2B8H10]2− anion to give formally closo isomeric 1-(arene) and 1-(cyclopentadiene)-1,2,4- and 1,2,3-metalladicarbaundecaboranes, and some substituent chemistry. Chiral separations, and crystal and molecular structures of [5-Br-1-(η6-C6Me6)-1,2,4-RuC2B8H9] and [2-Me-1-(η5-C5Me5)-1,2,3-RhC2B8H9]. Journal of Organometallic Chemistry 2000, 614-615, 269. <https://doi.org/10.1016/S0022-328X(00)00615-X>
  • Plešek Jaromı́r: The age of chiral deltahedral borane derivatives. Inorganica Chimica Acta 1999, 289, 45. <https://doi.org/10.1016/S0020-1693(99)00056-0>
  • Grüner Bohumı́r, Holub Josef, Plešek Jaromı́r, Vaněk Tomáš, Votavová Hana: High-performance liquid chromatographic enantiomeric resolution in the ten-vertex carborane series. Journal of Chromatography A 1998, 793, 249. <https://doi.org/10.1016/S0021-9673(97)00904-7>
  • Grüner Bohumir, Cisařová Ivana, Franken Andreas, Plešek Jaromı́r: Resolution of the [6,6′-μ-(CH3)2P-(1,7-(C2B9H10)2)-2-Co] bridged cobaltacarborane to enantiomers pure by chiral HPLC, circular dichroism spectra and absolute configurations by X-ray diffraction. Tetrahedron: Asymmetry 1998, 9, 79. <https://doi.org/10.1016/S0957-4166(97)00605-8>
  • Millan Mitchel D, Davis James H: Hydroboration of (1 R )-(+)-α-pinene and (1 S )-(−)-β-pinene with B 10 H 12 (SMe 2 ) 2 : a straightforward approach to the preparation of optically active 6-(alkyl)- nido -B 10 H 13 derivatives. Tetrahedron: Asymmetry 1998, 9, 709. <https://doi.org/10.1016/S0957-4166(98)00021-4>
  • Grüner Bohumir, Plzák Zbyněk: High-performance liquid chromatographic separations of boron-cluster compounds. Journal of Chromatography A 1997, 789, 497. <https://doi.org/10.1016/S0021-9673(97)00497-4>
  • Wang P, Lee H.K: Recent applications of high-performance liquid chromatography to the analysis of metal complexes. Journal of Chromatography A 1997, 789, 437. <https://doi.org/10.1016/S0021-9673(97)00839-X>