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Collect. Czech. Chem. Commun. 1985, 50, 343-347

Assignment techniques for 29Si NMR chemical shifts in pertrimethylsilylated products. Tests of empirical assignment rules by a modified 29Si indor

Jan Schramla, Michail Fedorovich Larinb and Vadim Aleksandrovich Pestunovichb

a Institute of Chemical Process Fundamentals, Czechoslovak Academy of Sciences, 165 02 Prague 6-Suchdol, Czechoslovakia
b Institute of Organic Chemistry, Siberian Branch of Academy of Sciences U.S.S.R., 664 033 Irkutsk, U.S.S.R.

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  • Harket Mouna, De Jeso Bernard, Lartigue Jean-Claude, Petraud Michel, Ratier Max: Application of the 29Si NMR 2D INEPT spin-flip J-resolved technique to the structural analysis of trimethylsilylated glycosides. Carbohydrate Research 1994, 263, 155. <>
  • Schraml Jan: 29Si N M R spectroscopy of trimethylsilyl tags. Progr Nucl Magn Reson Spectrosc 1990, 22, 289. <>
  • Pelnaƙ Jan, Blechta Vratislav, Schraml Jan: Functional Group Identification by Two-Dimensional 29Si NMR Spectroscopy with Reversed Detection and Signal Winnowing. Appl Spectrosc 1990, 44, 396. <>
  • Schraml Jan., Blechta Vratislav., Kvicalova Magdalena., Nondek Lubomir., Chvalovsky Vaclav.: Polar functional group analysis of mixtures by silicon-29 nuclear magnetic resonance. Anal. Chem. 1986, 58, 1892. <>
  • LaCourse Diane L., Jensen Trescott E.: Determination of 1-nitropyrene in extracts of vehicle particulate emissions. Anal. Chem. 1986, 58, 1894. <>
  • Past J., Puskar J., Alla M., Lippmaa E., Schraml J.: Selective heteronuclear INADEQUATE as an assignment technique: Applications to29Si-13C couplings in pertrimethylsilylated products. Magn. Reson. Chem. 1985, 23, 1076. <>