Collect. Czech. Chem. Commun. 1979, 44, 2507-2510
https://doi.org/10.1135/cccc19792507

Arylhydrazones of 5-nitrofurfuryl dichloromethyl sulfone

Adolf Jurášek, Jaroslav Kováč and Mária Bencková

Department of Organic Chemistry, Slovak Institute of Technology, 880 37 Bratislava

Abstract

X-Phenylhydrazones of α-dichloromethylsulfonyl-5-nitro-2-furaldehydes (X = H, 4-CH3, 4-OCH3, 4-Cl, 4-Br, 4-COOC2H5, 4-COOH, 4-NO2, 3-NO2) were prepared by condensation of aryldiazonium salts with 5-nitrofurfuryl dichloromethyl sulfone in ethanolic sodium acetate. IR, UV and 1H NMR spectra of the synthesized substances were interpreted.